Cold Gas Dynamic Manufacturing

Cold gas dynamic manufacturing (CGDM) is a new production process that enables novel combinations of materials and metals in a single 3D component. Using this technique, materials with previously unimaginable characteristics can be produced with relative ease.

 

Aims

  • Develop a system for the manufacture of metallic components by supersonic cold deposition of polymer, metal and ceramic powders
  • Establish a 'Cold Spray' capability
  • Move from a coating technique to a solid free form process and system integration
  • Demonstrate industrial applicability and pursue collaborative partnerships

The process

Cold gas dynamic spraying uses high-pressure, high-flow rate helium gas, heated to relatively low temperatures (150°-300°C). By using a supersonic converging/diverging nozzle, powder entrained in the high speed gas jet is accelerated to velocities in excess of 500-1000m/s. As the particles hit the target surface they impact under large plastic deformations, consolidating to produce localised forge bonding, depositing coatings at up to 100 g/min.

 

A bespoke manufacturing system has been designed for the cold spray process. The gas delivery system incorporates a world first flexible helium recycling plant developed by BOC gases. The design of particle acceleration nozzles is fundamental to the process and fluid dynamic simulations are used to optimise nozzle designs.

 

The CGDM system developed at the University of Cambridge is designed specifically for additive fabrication. While exploiting Cold Spray's high build rates, in-process machining was combined with novel build strategies to increase shaping fidelity. Moreover, helium was used as process gas to improve deposition performance and material functionality. To ensure economic viability, helium recycling was employed.

 

CGDM process schematic

 

CGDM rig

CGDM chamber

 

Areas of research

One of main areas of research in the CGDM project was nozzle design and bow shock phenomena; and in particular, how they affect deposition performance. In terms of nozzle design, Computational Fluid Dymanics (CFD) has been used extensively to help construct nozzles of different profile and length, specifically for the process. In order to assess their gas-dynamic performance, as well as to validate the CFD, Schlieren imaging and Particle Image Velocimetry (PIV) have been used to investigate gas flow and particle velocities respectively.

 

 

CGDM nozzle

Schlieren image showing nozzle exi

                

Images from PIV showing a) snapshot of powder stream b) snapshot overlaid with velocity vectors c) velocity distribution map

 

Results

We have successfully deposited aluminium, copper and titanium metal onto a variety of substrates of metal, ceramic, glass and plastic (including carbon reinforced composites). The deposits range in thickness from microns to several tens of millimeters.

 

Tri-material sandwich built up from aluminium, copper and titanium.

 

Notable achievements include:

  • several patent applications for a new method of producing inter-metalics
  • a world first in the design and realisation of CGDM with a fully integrated helium recycling system

 

A useful measure of deposition performance is deposition efficiency (DE), which is the ratio between the amount of powder deposited and the total amount of powder sprayed. It has been shown that both nozzle length and nozzle profile have significant impact on particle velocity and hence deposition performance. DEs in excess of 95% have been achieved when spraying aluminium, copper and titanium.

 

It has also been shown that the bow shock - formed at the impingement zone - has a negative influence on DE as a result of its effect on particle velocity; the high-density stagnation bubble can lead to particle deceleration. Since the strength of the bow shock is strongly dependent on standoff distance (SoD), as a result of the falling gas velocity outside the nozzle, three distinct SoD regions have been identified that affect deposition performance:

Diagram of the impingement zone

  • The short SoD region where the presence of the bow shock adversely affects deposition performance via a reduction in particle velocity. Here the DE rises rapidly until the influence of the bow shock becomes negligible.
  • The medium SoD region where particle velocity and DE may continue to increase if the gas velocity remains above the particle velocity and the DE is not already at 100%. Otherwise the DE begins to level off.
  • The high SoD region where the gas velocity has fallen below the particle velocity. If the particle velocity is at or close to the critical velocity then DE will begin to decrease.

Schlieren photographs of the bow shock at different standoff distances

 

 

Applications

  • The applications of CGDM span a range of industrial sectors including aerospace, biomedical, electronics and automotive
  • Metal coatings onto metal, glass, ceramics and plastics for electrical or heat conduction, brazing, corrosion and wear protection
  • Smart materials - embedded devices
  • Mould and tool repair and manufacture
  • Near-net powder metallurgy - spraying into moulds

Publications 

  • J. Pattison, S. Celotto, R. Morgan, M. Bray and W. O'Neill, Cold gas dynamic manufacturing: A non-thermal approach to freeform fabrication, International Journal of Machine Tools & Manufacture, 2007.47(3-4): p. 627-634.
  • J. Pattison, S. Celotto, R. Morgan and W. O'Neill,Cold spray nozzle design and performance evaluation using particle image velocimetry, International Thermal Spray Conference, Basel, Switzerland (2005).
  • R. Morgan, C. Sutcliffe, J. Pattison, M. Murphy, P. Fox and W. O'Neill,Analysis of cold gas dynamically sprayed aluminium deposits, Materials Letters, 58, pp1317-1320 (2004).

Collaborators

BOC Gases

BAE Systems

Qineti Q

Praxair

GKN

Stryker

 

Researchers

M. Bray

A. Cockburn

W. O'Neill

J. Pattinson

S. Celotto

 

Funding

EPSRC

 

Duration

2001 - 2007

 

 

 

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